GC/MS analysis results for sample AE11415, May 28 2002

NYC 9/11 Public Portal Document —p ulI LpL

Data File : C:\MSDCHEM\1\DATA\051702\11414.D Vial: 23 Acq On : 18 May 2002 7:32 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 2-Propenal, 3-(3,4-dimethox... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.28 ug/L 300525 Phenant hranerie-d10 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 2 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 45 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 4 Anthracene, 2-methyl- Abundance 192 C15H12 Scan 3319 (22.580 min): 11414.D (-3308) (-) 000613-12-7 42 m/z 192.10 100.00% 70) 1912

5000

40 82 96 70 I ' | 1 I I I | I I । ! J > . 120 146 160 > I I I ■ I I I I I I I I I I I I I I I > ■ I I I I I I I I I I I > I I I I I t > 1 P -T । i ■ ■ - ■ i ■ ■ ■ ■ i ■ ■ 22.20 22.40 22.60 22.80 23.00 m/z 191.10 1 21.35% 0 ■ r 1" i11'11 ■1 " i1 " 11'1111" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyI)- 192 161

5000 22.20 22.40 22.60 22.80 23.00 77 121 149 177 m/z 146.10 16.05% 91 103 A 138 52 64 1 ...I, I. '... ..I,... n/z-> O+ ilassgli...|... 1 11111' r ' ■ ‘ i1 +TT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ' i " " I

Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 192 164 210..... ..4 22.20 22.40 22.60 22.80 23.00 5000 99 m/ z 96.00 12.89% 115 47 77 177 67 125,34 146 mfe-> 0 +2738457 +7++ A n ,il7,11155., — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ’ITT

Abundance #125849: Anthracene, 9-methyl- 192 22.20 22.40 22.60 22.80 23.00 m/z 193.00 12.79% 5000

96 165 28 39 51 63 74 83 I 105 115 126 139 152 1 176 0 1 I I I 1‘I [-1 I I i’p I r I |‘| I I I I I1!1! |-| I I'ri i'Pi "I’rrl f| III I p-11! । [ । । 1 । । । । r’ I IJ I I‘l | | 1 ] i1! 1 I | | ill | 1 | i1! T-p-r ' i ' ■ ■ 1 i 1 ■ 1 1 i ■ ■ 1 1 i ' m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

11414.D 050102.M Tue May 21 15:57:11 2002 Page 8

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