GCMS analysis results for sample AE11156, May 2002

NYC 9/11 Public Portal Document LiDrary Searcn compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11156.D Vial: 22 Acq On : 16 May 2002 8:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.65 0.60 ug/1 48458 1,4-Dichlorob'enzene-d4 11.38 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

- 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 96 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 38 3 Allyl mercaptan 74 C3H6S 000870-23-5 27 4 Thiirane, methyl- 74 C3H6S 001072-43-1 16 Abund: Scan 97 (3.649 min): 11156. D (-93) (-) m/z 74.00 100.00% 74 82 5000 47 - r3.40 .....3.60 MY 3.80 4.00"Pro I I | I I !

...... 1 88 1 ' i ' ' ' ' i ' 1 ' 109i ' ■ ■ ■ i m/z 82.00 60.24% 113 /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

82 N । 1 | $4 1 1 , 5000 47 3.40 3.60 3.80 4.00 m/z 84.00 39.30% 35

m/z—> 12 26 | ,|| 1 1 I 1 1 1 1 i ' I’l’i I 1 1 ' । I 1 10 20 30 40 -2 50 60 — 1 70 80 , 90 TIil 108 111 > 1 > 11 ■ । ■ । ■ । ■ > > 11 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 1 ■ i ■ 1 ■ ■ i ■ ■ 1 ‘ i ■ 1 3.40 3.60 3.80 4.00 5000 82 m/ Z 76.10 34.52% 47

1‛I—B—mBBn—, 1 n11111' ' ' i ' ’ ' ■ I 1 1 1 1 I 1 ' ' 1 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 41 #28161: Allyl mercaptan 74 A _ W, . . .» —IT ■ ' i ■ ' 1 ' i ' ' ' ■ i ‘ ' 3.40 3.60 3.80 4.00 m/z 46.95 30.16% 5000

47 59 Ro । UWMMW.V/aoo mfz-> 27 33 , ----- 10 20 30 11153 40 50 60 II ■ ■ ■ 1 i1 70 ' ' i ■ ' ' ' i 1 ■ ' • i ■ ' ■ ■ i ' ' ' ■ i 80 90 100 110 3.40 3.60 3.80 4.00

11156.D SCAN020507.M Thu May 16 09:37:08 2002 Page 4

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