GCMS analysis results for sample AE11156, May 2002

NYC 9/11 Public Portal Document LLDLCLY oeuruii COILpOLIC nepox L

Data File : C:\MSDCHEM\l\DATA\020515\11156.D Vial: 22 Acq On : 16 May 2002 8:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.12 1.17 ug/1 93724 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 59 2 Butanoic acid, 3-oxo-, 2,2,2-tri... 232 C6H7C13O3 058547-15-2 12 3 Ethanimidamide, N-(l-amino-2,2,2... 303 C4H3C16N3 067172-64-9 12 4 N-Acetylpyrrolidone_________________ 127 C6H9NO2 000932-17-2 10 Abundance Scan 518 (6.123 min): 11156.D (-511) (-) m/ z 43.10 100.00% 43

5000 C 5.80 6.00 6.20 6.40 .... .. ................ . .... m/z 125.00 10.41% mfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 • • । ■ • ■ • । • ■ ■ ■ । 5.80 6.00 6.20 6.40 m/ z 83.00 7.85% 15 I 29 . , 63 83 97 125 TTr Pri , l 1" . . .”1 < < । > । । । | i ■ । । । । , । < j , > । । । ■ > > > । i । । । । i i । । । itti yri ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1068: Butanoic acid, 3-oxo-, 2,2,2-trichloroethyl ester 31 A. 1 1 1 11111d1 ' I 5.80 6.00 6.20 6.40 5000 m/z 47.00 7.31% 85 69 49

PTTr r, , . , r q 131 1801। .113 r, , :, । ..... , , v, । , 153 , । । i.। । । । , । । । । 234 । ri । i , । । । । t । । । । r । । । । । m/z-> Abundance 20 40 60 100 120 140 160 180 200 220 240 260 280 300 #3937: Ethanimidamide, N-(1-amino-2,2,2-trichloroethyliden... WNApLw 110 — Wiskolpoy 43 5.80 6.00 6.20 6.40 m/z 49.05 6.39% 5000 28

62 82 186 MMAphsahpvoalp . I I1109,23 l ll '.. 151 .... 137 Jl 171 1200 243 305 1 ■ ■ i ■ ‘ i'11'1 111,:1‘‘0111"011111000111123—3 1' • I ■''i'111i111। । > 11, > ।। > m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 5.80 6.00 6.20 6.40

11156.D SCAN020507.M Thu May 16 09:37:08 2002 Page 5

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