GCMS analysis results for sample AE11152, May 2002

NYC 9/11 Public Portal Document ulDrary searen compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11152.D Vial: 18 Acq On : 16 May 2002 4:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Acetonitrile, dichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.64 0.42 ug/1 33580 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

<1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 38 2 Allyl mercaptan 74 C3H6S 000870-23-5 12 3 Thiirane, methyl- 74 C3H6S 001072-43-1 9 4 3,3-/Dichloropropyne _________________ 108 C3H2C12 1000222-23-9 9 Abundance / Scan 96 (3.643 min): 11152.D (-91) (-) m/z 74.00 100.00% 74 82 5000 47 - MAM, l> 1 35 39

n/z—> 15 - 20 25 30 35 + —TPT 44 , 50 40 45 50 55 60 65 70 59 65 । d 1 " I' 75 80 ।1 ■111 ‘■ । 85 90 95 3.20 m/z 3.40 3.60 82.00 3.80 4.00 58.04% Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 | A It 1M440. 3.20 MPMAAA,AM, 41119: 3.40 3.60 3.80 4.00 38 47 m/z 47.05 36.17%

U - 86 ' I ■' ■111''111 ’ ‘' 111 ‘II‘ I " " I' " ' I vfz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 41 #28161: Allyl mercaptan 74 AW/w 3.20 3.40 3.60 3.80 4.00 5000 m/z 84.00 34.65% 45

n/z-> 15 42427,33, 1 45IM50 535556 5960 65 687071 75 80 85 90 95 20 25 30 35 40 t 11 11 m 111111111111111111 n 1111 11■1■ i ■'11111" i111' i tMuwd Abundance #115343: Thirane, methyl- 411 74 3.20 3.40 3.60 3.80 4.00 m/z 76.00 31.65% 5000 45

m/z—> ■ ।11 ■11 ■ 15 20 +247257.30393335 1 40 445 TTp 18 50 53,5651,.6468711477— r-1111 *1" i MAA 55 60 65 70 75 80 85 90 95 3.20 3.40 3.603.80 4.00

11152.D SCAN020507.M Thu May 16 09:28:34 2002 Page 3

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