GCMS analysis results for sample AE11303, May 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\l\DATA\020516\11303.D Vial: 14 Acq On : 16 May 2002 10:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.64 0.41 ug/1 22312 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 2 3,3 -Dichloropropyne 108 C3H2C12 1000222-23-9 25 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 Thiirane, methyl- 74 C3H6S 001072-43-1 7 Abundance f Scan 96 (3.643 min): 11303.D (-91) (-) m/ z 74.00 100.00% 74

5000 82 - 35 47

LllH mm 3.20 3.40 3.60 3.80 4.00 i" " r i ■'1 ‘ i1 T’IIT 11"' t" " r "' r " ■ i', ri i'" 11 > 111 m/z 82.00 45.30% n/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #115342: Acetonitrile dichloro- 74 35

5000 82 3.20 3.40 3.60 3.80 4.00 47 m/z 83.95 38.44%

m/z—> Abundance i ■ ■ ■11'"' i1'" i''' I ll l [ITT) | ■ ■ >> f ■ l ■ ■ | l 1 I ■ |] 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 #28312:3,3-Dichloropropyne TTTp- 11 , 11 11 111 । i i! iq-r i r i ।. 11 . ।, 11 111 , ( MpHWlaypoot. 74 3.20 3.40 3.60 3.80 4.00 5000 m/z 76.00 31.52% 38 47 28 TWTTTTTTTTTTpTT —.53,.S0. 82 108 n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #28161: Allyl mercaptan 41 74 3.20 3.40 3.60 3.80 4.00 m/z

wAh 47.10 22.65% 5000

27 33 । 47 Mlpk n/z-> mH 11 53 59 69, | , 111 1111111111111111111111111111 1111111 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 " r "11"" r "' i"" i""i""i 3.20 3.40 3.60 3.80 4.00

11303.D SCAN020507.M Fri May 17 13:09:44 2002 Page 3

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