GC/MS reference analysis results, sample AE09683, May 15 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY1002\REF2.D Vial: 5 Acq On : 10 May 2002 4:58 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 13 9:06 2002 Quant । Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 13 08:58:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.17 152 512884 40.00 ug/1 -0.03 10) Naphthalene-d8 15.79 136 1866623 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.11 164 1012594 40.00 ug/1 -0.03 30) Phenanthrene-diO 25.55 188 1400780 40.00 ug/1 -0.02 38) Chrysene-dl2 33.62 240 847281 40.00 ug/1 -0.02 44) Perylene-dl2 37.84 264 527775 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.24 209 152622 30.30 ug/L -0.03 Spiked Amount 40.000 Recovery 75.75%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.82 74 119883 9.28 ug/1 98 3) bis(2-Chloroethyl)ether 11.56 93 229763 13.71 ug/1 95 4) 1,3-Dichlorobenzene 12.07 146 193333 12.16 ug/1 95 5) 1,4-Dichlorobenzene 12.20 146 204549 11.76 ug/1 99 6) 1,2-Dichlorobenzene 12.73 146 198255 13.10 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.05 45 471569 14.52 ug/1 98 8) N-Nitrosodi-n-propylamine 13.43 70 166575 13.92 ug/1 96 9) Hexachloroethane 13.57 117 55656 9.00 ug/1 97 11) Nitrobenzene 13.84 77 191267 12.62 ug/1 98 12) Isophorone 14.48 82 471668 15.88 ug/1 99 13) bis(2-Chloroethoxy)methane 15.17 93 271179 14.09 ug/1 99 14) 1,2,4-Trichlorobenzene 15.68 180 165111 12.74 ug/1 99 15) Naphthalene 15.85 128 571979 14.89 ug/1 99 16) Hexachlorobutadiene 16.40 225 63062 10.51 ug/1 99 18) Hexachlorocyclopentadiene 18.60 237 12257 2.39 ug/1 98 19) 2-Chloronaphthalene 19.36 162 342382 15.48 ug/1 98 20) Dimethylphthalate 20.45 163 415904 14.93 ug/1 99 21) 2,6-Dinitrotoluene 20.67 165 60636 10.18 ug/1 96 22) Acenaphthylene 20.63 152 536382 13.61 ug/1 100 2 3) Acenaphthene 21.19 153 359643 15.31 ug/1 100 24) 2,4-Dinitrotoluene 21.83 165 69799 10.87 ug/1 96 25) Diethylphthalate 22.59 149 413589 16.58 ug/1 99 26) 4-Chlorophenylphenylether 22.74 204 181514 14.72 ug/1 99 27) Fluorene 22.71 166 392500 15.84 ug/1 99 29) Azobenzene 23.21 77 426863 13.82 ug/L 96 31) N-Nitrosodiphenylamine 23.13 168 139182 15.91 ug/1 97 32) 4-Bromophenylphenylether 24.21 248 99873 14.42 ug/1 99 33) Hexachlorobenzene 24.64 284 121343 15.33 ug/1 97 3 4) Phenanthrene 25.62 178 516246 15.36 ug/1 99

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0510.M Mon May 13 09:07:58 2002 Page 1

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