GCMS calibration results for volatile organics, May 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0902\CAL80.D Vial: 2 Acq On 9 May 2002 3:16 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 10:10 2002 Quant Results File: GCMS0507.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:50:49 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.19 152 469400 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1701036 40.00 ug/1 0.00 17) Acenaphthene-diO 21.14 164 916194 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1288195 40.00 ug/1 0.00 38) Chrysene-d12 33.65 240 830311 40.00 ug/1 0.00 44) Perylene-dl2 37.87 264 494874 40.00 ug/1 0.00 System Monitoring Compounds 28) TCMX 23.28 209 43814 9.61 ug/L 0.00 Spiked Amount 10.000 Recovery = 96.10% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.84 74 926614 78.37 ug/1 98 3) bis(2-Chloroethyl)ether 11.59 93 1203952 78.51 ug/1 96 4) 1,3-Dichlorobenzene 12.09 146 1150823 79.12 ug/1 98 5) 1,4-Dichlorobenzene 12.24 146 1255218 78.87 ug/1 99 6) 1,2-Dichlorobenzene 12.75 146 1095091 79.06 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.07 45 2299541 77.35 ug/1 98 8) N-Nitrosodi-n-propylamine 13.47 70 850636 77.65 ug/1 97 9) Hexachloroethane 13.61 117 447632 79.06 ug/1 90 11) Nitrobenzene 13.88 77 1115169 80.74 ug/1 96 12) Isophorone 14.52 82 2148071 79.35 ug/1 98 13) bis(2-Chloroethoxy)methane 15.21 93 1393960 79.48 ug/1 100 14) 1,2,4-Trichlorobenzene 15.72 180 947619 80.24 ug/1 99 15) Naphthalene 15.90 128 2785526 79.58 ug/1 99 16) Hexachlorobutadiene 16.44 225 443250 81.08 ug/1 99 18) Hexachlorocyclopentadiene 18.63 237 383200 82.53 ug/1 100 19) 2-Chloronaphthalene 19.40 162 1590412 79.46 ug/1 98 20) Dimethylphthalate 20.50 163 1996832 79.23 ug/1 100 21) 2,6-Dinitrotoluene 20.72 165 460594 85.44 ug/1 91 22) Acenaphthylene 20.67 152 2813270 78.87 ug/1 99 2 3) Acenaphthene 21.24 153 1670729 78.58 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 508366 87.49 ug/1 89 25) Diethylphthalate 22.63 149 1786157 79.13 ug/1 100 26) 4-Chlorophenylphenylether 22.78 204 899940 80.66 ug/1 97 27) Fluorene 22.76 166 1785889 79.66 ug/1 100 29) Azobenzene 23.25 77 2130960 76.25 ug/L 95 31) N-Nitrosodiphenylamine 23.17 168 644770 80.13 ug/1 91 32) 4-Bromophenylphenylether 24.24 248 515880 80.98 ug/1 97 33) Hexachlorobenzene 24.68 284 589361 80.98 ug/1 98 34) Phenanthrene 25.66 178 2467683 79.84 ug/1 100 (#) = qualifier out of range (m) = manual integration CAL80.D GCMS0507.M Fri May 10 10:10:43 2002 Page 1

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