GCMS reference data for sample AE10431, May 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY1002\REFB2.D Vial: 27 Acq On : 11 May 2002 3:28 pm Operator : Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 16 9:47 2002 Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 16 09:35:44 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.16 152 431684 40.00 ug/1 -0.03 10) Naphthalene-d8 15.80 136 1552042 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.11 164 857159 40.00 ug/1 -0.03 30) Phenanthrene-diO 25.55 188 1200410 40.00 ug/1 -0.02 38) Chrysene-dl2 33.61 240 790683 40.00 ug/1 -0.02 44) Perylene-dl2 37.84 264 537485 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.24 209 37846 8.88 ug/L -0.03 Spiked Amount 10.000 Recovery = 88.80%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.83 74 108248 9.96 ug/1 97 3) bis(2-Chloroethyl)ether 11.56 93 231403 16.41 ug/1 96 4) 1,3-Dichlorobenzene 12.06 146 156490 11.70 ug/1 96 5) 1,4-Dichlorobenzene 12.21 146 167556 11.45 ug/1 99 6) 1,2-Dichlorobenzene 12.72 146 167856 13.18 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.04 45 476168 17.42 ug/1 99 8) N-Nitrosodi-n-propylamine 13.43 70 172985 17.17 ug/1 99 9) Hexachloroethane 13.57 117 46315 8.89 ug/1 95 11) Nitrobenzene 13.84 77 205254 16.29 ug/1 98 12) Isophorone 14.49 82 492849 19.95 ug/1 98 13) bis(2-Chloroethoxy)methane 15.18 93 276948 17.31 ug/1 99 14) 1,2,4-Trichlorobenzene 15.68 180 145727 13.52 ug/1 100 15) Naphthalene 15.86 128 548114 17.16 ug/1 100 16) Hexachlorobutadiene 16.40 225 53818 10.79 ug/1 99 18) Hexachlorocyclopentadiene 18.60 237 16655 3.83 ug/1 99 19) 2-Chloronaphthalene 19.36 162 338138 18.06 ug/1 99 20) Dimethylphthalate 20.46 163 424175 17.99 ug/1 100 21) 2,6-Dinitrotoluene 20.67 165 78211 15.51 ug/1 99 22) Acenaphthylene 20.63 152 533178 15.98 ug/1 100 23) Acenaphthene 21.20 153 355901 17.89 ug/1 100 24) 2,4-Dinitrotoluene 21.84 165 90116 16.58 ug/1 90 25) Diethylphthalate . 22.59 149 415728 19.69 ug/1 100 26) 4-Chlorophenylphenylether 22.74 204 177595 17.01 ug/1 99 27) Fluorene 22.72 166 394250 18.80 ug/1 100 29) Azobenzene 23.21 77 438672 16.78 ug/L 97 31) N-Nitrosodiphenylamine 23.13 168 136061 18.15 ug/1 94 32) 4-Bromophenylphenylether 24.20 248 98862 16.65 ug/1 96 33) Hexachlorobenzene 24.64 284 119328 17.59 ug/1 99 34) Phenanthrene 25.62 178 527797 18.32 ug/1 99

(#) = qualifier out of range (m) = manual integration REFB2.D GCMS0510.M Thu May 16 09:53:08 2002 Page 1

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