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GCMS calibration results for volatile organics, May 2002

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Laboratory report of gas chromatography mass spectrometry calibration data for volatile organic compounds conducted on May 9, 2002.

NYC-WTC_000023216–000023219

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document < uullU - L d L LULL repOrC (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY0 902\CAL8 0.D Vial: 2 Acq On 9 May 2002 3:16 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 10:10 2002 Quant Results File: GCMS0507.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:50:49 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.79 178 2572168 79.99 ug/1 100 36) Di-n-butylphthalate 27.56 149 3206072 80.38 ug/1 99 37) Fluoranthene 29.28 202 2487717 80.57 ug/1 97 3 9) Pyrene 29.95 202 2310729 82.57 ug/1 96 40) Butylbenzylphthalate 32.09 149 1184949 83.19 ug/1 92 41) Benzo(a)anthracene 33.59 228 1749347 81.05 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.87 149 1527297 80.85 ug/1 99 43) Chrysene 33.73 228 1723439 79.98 ug/1 100 45) Di-n-Octylphthalate 35.61 149 2201383 85.13 ug/1 # 95 46) Benzo(b)fluoranthene 36.71 252 1415607 79.79 ug/1 97 47) Benzo(k)fluoranthene 36.77 252 1387261 73.87 ug/1 98 48) Benzo(a)pyrene 37.69 252 1294704 80.76 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.98 276 1193001m 78.34 ug/1 50) Dibenz(a,h)anthracene 42.05 278 946916 78.04 ug/1 98 51) Benzo(g,h,i)perylene 43.21 276 934357 76.70 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0507.M Fri May 10 10:10:44 2002 Page 2

NYC-WTC_000023218

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NYC-WTC_000023218Source: NYC Law Department, mirrored locally

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