Laboratory report detailing analytical results for volatile organic compounds in sample AE07109 collected on March 26, 2002.
NYC-WTC_000022416–000022489Folder label: “524 3/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)
Data File : C:\HPCHEM\1\DATA\02mar26\0326R5A.D Vial: 4 Acq On : 26 Mar 2002 3:25 pm Operator: 201-wb Sample : ref 5• Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 26 16:04 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Mar 25 15:09:58 2002 Response via : Initial Calibration DataAcq Meth .: HP031802
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-DIFLUOROBENZENE 15.07 114 872871 5.00 ug/L 0.02 24) CHLOROBENZENE-D5 21.72 117 823827 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.90 152 464478 5.00 ug/L 0.02
System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.30 65 436665 6.07 ug/L 0.02 Spiked Amount 5.000 Recovery = 121.40% 3) 4-BROMOFLUOROBENZENE 24.31 174 370013 5.25 ug/L 0.02 Spiked Amount 5,000 Recovery = 105.00% 25) TOLUENE-D8 18.42 98 1009793 5.06 ug/L 0.02 Spiked Amount 5.000 Recovery = 101.20%
Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.84 85 71663 2.76 ug/L 98 5) CHLOROMETHANE 5.46 50 90957 2.99 ug/L 92 6) VINYL CHLORIDE 5.57 62 107260 4.86 ug/L 99 7) BROMOMETHANE . 6.55 94 82107 3.96 ug/L 92 8) CHLOROETHANE 6.68 64 86838 4.06 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.23 101 188925 4.34 ug/L 98 12) ACETONE 8.21 43 59134 8.38 ug/L 93 13) 1,1-DICHLOROETHENE 8.56 61 235139 4.51 ug/L 98 14) METHYLENE CHLORIDE 9.57 49 217294 4.69 ug/L 96 15) METHYL TERT BUTYL ETHER 9.88 73 238680 5.10 ug/L 96 16) TRANS-1,2-DICHLOROETHENE 10.23 61 227477 4.34 ug/L 99 17) 1,1-DICHLOROETHANE 11.13 63 277859 4.63 ug/L 96 18) 2-BUTANONE (MEK) . 11.97 43 32685 5.09 ug/L 99 19) 2,2-DICHLOROPROPANE 12.34 77 210940 4.63 ug/L 98 20) CIS-1,2-DICHLOROETHENE 12.45 96 153518 4.35 ug/L 96 21) CHLOROFORM 12.77 83 311031 4.79 ug/L 99 2 2) BROMOCHLOROMETHANE 13.14 49 109123 4.05 ug/L 99 23) 1,2 -DICHLOROETHANE . 14.51 62 237272 5.29 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.67 97 239692 5.15 ug/L 99 27) 1,1-DICHLOROPROPENE 14.00 75 177731 4.15 ug/L 97 28) CARBON. TETRACHLORIDE 14.25 117 209881 5.24 ug/L 97 29) BENZENE 14.59 78 470054 4.41 ug/L 98 3 0) TRICHLOROETHENE 15.87 95 154097 4.63 ug/L 98 31) 1,2-DICHLOROPROPANE 16.23 63 119010 4.28 ug/L 97 32) DIBROMOMETHANE 16.91 174 82978 5.26 ug/L 88 33) BROMODICHLOROMETHANE 16.74 83 220488 5.23 ug/L 97 34) 2-CHLOROETHYL VINYL ETHER 17.23 63 36727 3.31 ug/L 89 35) METHYL ISO-BUTYL KETONE 17.31 58 17819 3.75 ug/L 95 36) CIS-1,3-DICHLOROPROPENE 17.84 75 174970 ■ 4.34 ug/L 99 37) TOLUENE 18.59 91 516024 4.52 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 148677 4.99 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.26 97 90711 4.81 ug/L 96 40) TETRACHLOROETHENE 20.04 166 158459 4.69 ug/L 99 41) 1,3-DICHLOROPROPANE 19.78 76 156300 4.50 ug/L 96 42) DIBROMOCHLOROMETHANE 20.48 129 126162 5.18 ug/L 97 ■43) 1,2-DIBROMOETHANE 20.94 107 89345 4.65 ug/L 99 4 4) CHLOROBENZ ENE 21.81 112 361123 4.70 ug/L 95 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 143444 5.28 ug/L 97 46) 2-HEXANONE 19.15 43 47975 5.45 ug/L 93 47) ETHYLBENZENE 21.86 91 618069 4.66 ug/L 99 48) P & M-XYLENE 22.01 106 409755 9.05 ug/L 87 (#) = qualifier out of range (m) = manual integration 0326R5A.D HP031802.M Tue Mar 26 16:04:21 2002 Page 1
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