VOC analysis results, sample AE02575, Feb 8 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\02FEB08\0208C10C.D Vial: 4 Acq On 8 Feb 2002 4:58 pm Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 14 17:32 2002 Quant Results File: HP021102.RES Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 14 17:25:54 2002 Response via : Initial Calibration DataAcq Meth : HP020502

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.11 114 1837329 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.78 117 1817486 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.95 152 833666 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 698560 4.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.80% 3) 4-BROMOFLUOROBENZENE 24.36 174 656261 4.75 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.00% 25) TOLUENE-D8 18.47 98 2285272 5.07 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.40% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.89 85 811965 12.59 ug/L 100 5) CHLOROMETHANE 5.47 50 627050 12.76 ug/L 93 6) VINYL CHLORIDE 5.61 62 305426 15.05 ug/L 96 7) BROMOMETHANE 6.61 94 407275 12.39 ug/L 97 8) CHLOROETHANE 6.75 64 338448 10.74 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.30 101 741547 11.72 ug/L 97 11) 1,1,2-Trichloro-l,2,2-trif 8.20 101 388974 8.32 ug/L 94 12) ACETONE 8.27 43 118301 9.37 ug/L 95 13) 1,1-DICHLOROETHENE 8.62 61 753254 8.53 ug/L 97 14) METHYLENE CHLORIDE 9.63 49 1022268 9.63 ug/L 99 15) METHYL TERT BUTYL ETHER 9.93 73 949828 8.10 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.29 61 1081525 9.58 ug/L 96 17) 1,1-DICHLOROETHANE 11.18 63 1292355 9.68 ug/L 98 18) 2-BUTANONE (MEK) 12.02 43 313955 10.73 ug/L 98 19) 2,2-DICHLOROPROPANE 12.42 77 1060232 9.90 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.50 96 777769 10.20 ug/L 99 21) CHLOROFORM 12.83 83 1353616 10.09 ug/L 100 22) BROMOCHLOROMETHANE 13.22 49 621081 9.74 ug/L 100 23) 1,2-DICHLOROETHANE 14.56 62 870470 9.64 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.72 97 1033988 10.20 ug/L 100 27) 1,1-DICHLOROPROPENE 14.05 75 1056106 10.44 ug/L 99 28) CARBON TETRACHLORIDE 14.31 117 839776 10.19 ug/L 99 29) BENZENE 14.64 78 2649393 10.09 ug/L 99 30) TRICHLOROETHENE 15.93 95 822133 10.47 ug/L 98 31) 1,2-DICHLOROPROPANE 16.28 63 764781 10.31 ug/L 97 32) DIBROMOMETHANE 16.96 174 336453 9.55 ug/L 96 33) BROMODICHLOROMETHANE 16.80 83 975099 10.27 ug/L 100 34) 2-CHLOROETHYL VINYL ETHER 17.27 63 276349 10.07 ug/L 96 (#) = qualifier out of range (m) = manual integration 0208C10C.D HP021102.M Thu Feb 14 17:32:46 2002 Page 1

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