VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02feb06\0206C10B.D Vial: 3 Acq On 7 Feb 2002 12:27 am Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Feb 7 1:06 2002 Quant Results File: HP013102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Feb 01 13:18:32 2002 Response via : Initial Calibration DataAcq Meth : HP013102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.11 114 2242453 5.00 ug/L 0.00 2 4) CHLOROBENZENE-D5 21.76 117 2242918 5.00 ug/L 0.00 52) 1,4-DICHLOROBENZENE-D4 26.95 152 1041655 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 882168 4.54 ug/L 0.00 Spiked Amount 5.000 Recovery = 90.80% 3) 4-BROMOFLUOROBENZENE 24.36 174 847173 4.93 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.60% 25) TOLUENE-D8 18.47 98 2765332 4.94 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.80%

' Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.86 85 496237 12.95 ug/L 99 — 5) CHLOROMETHANE 5.49 50 492671 11.04 ug/L 97 — 6) VINYL CHLORIDE 5.59 62 238273 9.78 ug/L 98 — 7) BROMOMETHANE 6.59 94 329285 10.09 ug/L 97 — 8) CHLOROETHANE 6.73 64 310330 10.78 ug/L 94 — 9) TRICHLOROFLUOROMETHANE 7.30 101 613393 9.11 ug/L 94 — 10) Isopropyl Alcohol 7.85 45 2641 22.71 ug/L 74 “ 11) 1,1,2-Trichloro-1,2,2-trif 8.19 101 516532 10.32 ug/L 98 . 12) ACETONE 8.27 43 210909 17.43 ug/L 95 — 13) 1,1-DICHLOROETHENE 8.62 61 1135188 10.77 ug/L 99 — 14) METHYLENE CHLORIDE 9.63 49 1320422 12.66 ug/L 99 — 15) METHYL TERT BUTYL ETHER 9.93 73 1342488 10.24 ug/L 97 — 16) TRANS-1,2-DICHLOROETHENE 10.29 61 1363508 10.68 ug/L 96 17) 1,1-DICHLOROETHANE 11.18 63 1619931 10.52 ug/L 98 18) 2-BUTANONE (MEK) 12.01 43 405452 14.26 ug/L 99 19) 2,2-DICHLOROPROPANE 12.40 77 1092027 8.47 ug/L 100 _ 20) CIS-1,2-DICHLOROETHENE 12.50 96 957476 10.39 ug/L 96 — 21) CHLOROFORM 12.83 83 1668580 9.73 ug/L 97 — 22) BROMOCHLOROMETHANE 13.22 49 800357 10.85 ug/L 96 — 23) 1,2-DICHLOROETHANE 14.56 62 1148175 9.49 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.72 97 1255020 8.82 ug/L 99 — 27) 1,1-DICHLOROPROPENE 14.05 75 1280252 10.08 ug/L 99 28) CARBON TETRACHLORIDE 14.31 117 1028264 8.88 ug/L 99 — 29) BENZENE 14.64 78 3247315 10.38 ug/L 99 — 30) TRICHLOROETHENE 15.91 95 1009911 9.70 ug/L 99 - 31) 1,2-DICHLOROPROPANE 16.28 63 956495 10.47 ug/L 99 — 32) DIBROMOMETHANE 16.94 174 458526 9.39 ug/L 92 —= 33) BROMODICHLOROMETHANE 16.80 83 1224431 8.89 ug/L 99--

(#) = qualifier out of range (m) = manual integration 0206C10B.D HP013102.M Thu Feb 07 01:06:16 2002 Page 1

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