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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.

NYC-WTC_000019130–000019152

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHQDS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF' Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.617 276 280 292 rBV 259211 767028 9.58% 1.592% 2 11.133 659 663 678 rBV 42528 113268 1.41% 0.235% 3 11.674 717 722 747 rBV 1976091 5447422 68.04% 11.306% 4 14.309 998 1009 1019 rBV 525037 1127970 14.09% 2.341% . 5 15.282 1109 1115 1135 rBV 2660526 6734534 84.12% 13.978%

6 17.449 1345 1351 1361 rBV 1110576 2455090 30.67% 5.096% 7 18.156 1423 1428 1437 rBV 103557 222372 2.78% 0.462% 8 20.276 1653 1659 1668 rBV 866741 1839799 22.98% 3.819% 9 20.561 1683 1690 1707 rBV 3194444 7527601 94.02% 15.624%' 10 21.029 1737 1741 1762 rBV 211917 798829 9.98% 1.658%

11 22.792 1927 1933 1941 rBV 570534 1218559 15.22% 2.529% 12 24.986 2163 2172 2204 rBV3 2585894 8006049 100.00% 16.617% 13 26.886 2373 2379 2387 rVB 303698 656163 8.20% 1.362% 14 28.658 2566 2572 2580 rVB 238504 540647 6.75% 1.122% 15 30.062 2720 2725 2735 rBV 276978 627924 7.84% 1.303%

16 30.246 2739 2745 2755 rVB 208692 487401 6.09% 1.012% 17 31.715 2899 2905 2916 rVB 179568 430423 5.38% 0.893% 18 33.028 3041 3048 3074 rBV 1731861 5346097 66.78% 11.096% 19 34.377 3188 3195 3204 rBV 100867 307994 3.85% 0.639% 20 35.571 3319 3325 3335 rBV 68154 209319 2.61% 0.434%

21 36.718 3442 3450 3457 rBV2 38678 128274 1.60% 0.266% 22 37.122 3486 3494 3514 rBV2 912881 3186934 39.81% 6.615%

Sum of corrected areas: 48179697

30256.D GCMS1126.M Wed Jan 02 10:23:57 2002

NYC-WTC_000019135

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NYC-WTC_000019135Source: NYC Law Department, mirrored locally

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