GCMS calibration table, sample AD31129, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C: \HPCHEM\ 1 \DATA\JANO 902\31129A.D Vial: 26 Acq On : 10 Jan 2002 3:31 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 8:51 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table . j Last Update : Thu Dec 13 14:40:46 2001 — V J - Response via : Initial Calibration JC J ( U DataAcq Meth : GCMS0103 I A V )9

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Di chlorobenzene -d4 11.52 152 935195 20.00 ug/1 0.00 10) Naphthalene-d8 15.12 136 3655595 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1851057 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2579030 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1434229 20.00 ug/1 0.00 44) Perylene-dl2 36.91 264 830269 20.00 ug/1 0.01

System Monitoring Compounds 37) 2,4-DDD 29.88 235 102611 3.47 g/mL -0 Spiked Amount 5.000 Recovery .69.40%

Target Compounds Qva .e 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 13.40 82 100 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 1514 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.82 165 175 N.D. 25) Diethylphthalate 21.91 149 666 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31129A.D GCMS0103.M Wed Feb 06 08:51:41 2002 Page 1

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