NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN0902\31130A.D Vial: 27
Acq On : 10 Jan 2002 4:30 pm Operator: 209 GALOS
Sample : gems scan 12/21 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 6 8:49 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Thu Dec 13 14:40:46 2001
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 900956 20.00 ug/1 0.00
10) Naphthalene-d8 15.12 136 3506869 20.00 ug/1 0.00
17) Acenaphthene-diO 20.39 164 1775151 20.00 ug/1 0.00
29) Phenanthrene-diO 24.81 188 2492569 20.00 ug/1 0.00
38) Chrysene-dl2 32.84 240 1463037 20.00 ug/1 0.00
44) Perylene-dl2 36.91 264 823917 20.00 ug/1 0.01
System Monitoring Compounds
37) 2,4-DDD 29.88 235 102338 3.58 ug/mL -0.19
Spiked Amount 5.000 Recovery = 71.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.11 74 124 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 12.87 77 103 N.D.
12) Isophorone 13.41 82 542 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.19 128 1442 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.85 165 188 N.D.
25) Diethylphthalate 21.92 149 1112 N.D.
26) 4-Chioropheny1-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31130A.D GCMS0103.M Wed Feb 06 08:50:02 2002 Page 1
NYC-WTC_000019006
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