GC/MS analysis results for sample AD30905, Jan 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.Data File C:\HPCHEM\1\DATA\DEC3101\30905.D Vial: 45 Acq On 2 Jan 2002 7:33 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.75 0.73 ug/1 206758 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 1-Octadecanol 270 C18H380 000112-92-5 9 3 Ethene, chloro- 62 C2H3C1 000075-01-4 9 4 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 Abundance Scan 295 (7.755 min): 30905.D (-) m/z 4 .95 100.00% 43

5000

61 82 97 125 7.40 7.60 7.80 8.00 • I » I ■ 1 I IAh.Tr1..’ ■ J.t Htt.____ Il t1-t3*1*1*11** ’ »» I I - 111*1*t*t1-1111Tr**111111111111111I m/z 46.90 8.16% m/z-> 20 40> 60 80 100 120 140 160 180 200 220 240 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43 MNMWa MAwoA 5000 T IT 7.40 7.60 ' 7.80 8.00 15 m/z 124.85 7.55% ! 85 97 125 I —IIPPIT 1ada-0da 01**1* miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance । #72026; 1-Octadecanol i 43 55 • ■ i ■ ■ ■ ■ i ■ ■ • ■ i ' ■ ■ ■ i ■ ■ ■ • i ■ 7.40 7.60 7.80 8.00 5000 83 m/z 126.90 7.55% 71 ! 97 27 | 111 125 224 252 miz-> 20 40 60 80 100 120 140 160 180 200 220 240’ Abundance #135: Ethene, chloro- * ' I ’ ’ ‘ ‘ ‘ ‘ ' I ’ ' ’ ’ ! ' 1 ‘ * I ‘ 27 7.40 7.60 7.80 8.00 62 m/z 81.95 7.21% 5000

vn!z~> -A4 80 100 120 140 160 180 200 220 240 20 40 60 ‘ ■ i ■ ■ • ‘ i1 • ■ • i • ■ ■ • i ■ ■ • ■ i ■ • ■ ■ i • • ■ ■ i ■ ■ ‘ ■ i ■1 ■ ‘ i1 ■ ■ • । 7.40 7.60 7.80 ' ‘ I 1 1 ' ' t ' 8.00

30905.D GCMS1126.M Fri Jan 25 11:31:08 2002 Page 2

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