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GCMS calibration results for sample AD30643, Feb 2002

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Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018436–000018439

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File M:\INSTRU~1\2 0 9\DATA\DEC2 7 01\CAL4 0A.D Vial: 2 Acq On 30 Dec 2001 11:12 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 31 16:22 2002 . Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.62 168 1785836 39.44 ug/1 94 31) 4-Bromophenyl-phenylether 23.67 248 982581 39.16 ug/1 98 3 2) Hexachlorobenzene 24.09 284 1125240 40.78 ug/1 98 3 3) Phenanthrene 25.06 178 5269865 39.01 ug/1 100 34) Anthracene 25.20 178 5105533 37.92 ug/1 99 35) Di-n-butylphthalate 27.00 149 7316676 40.70 ug/1 99 36) Fluoranthene 28.68 202 5273712 40.44 ug/1 98 3 9) Pyrene 29.34 202 5355168 36.11 ug/1 97 40) Butylbenzylphthalate 31.51 149 2876478 37.14 ug/1 98 41) Benzo(a)anthracene 32.99 228 3833197 37.44 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 3706301 35.41 ug/1 99 43) Chrysene 33.11 228 3808564 37.93 ug/1 100 45) Di-n-Octylphthalate 35.04 149 5604193 38.75 ug/1 99 46) Benzo(b)fluoranthene 36.07 252 3062002 37.40 ug/1 99 47) Benzo(k)fluoranthene 36.13 252 3298131 39.25 ug/1 99 48) Benzo(a)pyrene 36.96 252 2700915 37.94 ug/1 98 49) Indeno(l,2,3-cd)pyrene 40.83 276 2477674 34.81 ug/1 98 50) Dibenz(a,h)anthracene 40.88 278 1945201 34.90 ug/1 99 51) Benzo(g,h,i)perylene 41.93 276 1980313 32.56 ug/1 100

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS1126.M Thu Jan 31 16:23:39 2002 Page 2

NYC-WTC_0000 18438

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NYC-WTC_000018438Source: NYC Law Department, mirrored locally

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