GCMS calibration results for sample AD30643, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File M:\INSTRU-1\2 09\DATA\DEC27 01\CAL4 0A.D Vial: 2 Acq On 30 Dec 2001 11:12 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 31 16:22 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title •: 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 884495 20.00 ug/1 -0.02 10) Naphthalene-d8 15.29 136 3443916 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 1692117 20.00 ug/1 -0.01 2 9) Phenanthrene-dl0 24.99 188 2550704 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1718209 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1088404 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.44 74 1791299 46.05 ug/1 97 3) bis(2-Chloroethyl)ether 11.12 93 2626508 43.02 ug/1 99 4) 1,3-Dichlorobenzene 11.58 146 2502840 38.91 ug/1 100 5) 1,4-Dichlorobenzene 11.72 146 2538607 39.03 ug/1 99 6) 1,2-Dichlorobenzene 12.24 146 2337065 38.96 ug/1 99 7) 2,2’-oxybi s(1-Chioropropan 12.58 45 4051897 “ 11 ug/1 98 8) N-Nitroso-di-n-propylamine 12.98 70 1739841 02 ug/1 99 9) Hexachloroethane 13.06 117 1026116 43.37 ug/1 100 11) Nitrobenzene 13.37 77 2647467 49.32 ug/1 100 12) 1sophorone 14.02 82 4769048 46.11 ug/1 99 13) bis(2-Chloroethoxy)methane 14.70 93 3027020 43.57 ug/1 100 14) 1,2,4-Trichlorobenzene 15.18 180 1916802 38.33 ug/1 99 15) Naphthalene 15.35 128 6540167 39.74 ug/1 100 16) Hexachlorobutadiene 15.89 225 992074 40.71 ug/1 99 18) Hexachlorocyclopentadiene 18.07 237 331154 2716 ug/1 99 19) 2-Chloronaphthalene 18.84 162 3709308 38.43 ug/1 99 20) Dimethylphthalate 19.96 163 4350646 38.69 ug/1 100 21) 2,6-Dinitrotoluene 20.17 165 1036309 39.00 ug/1 97 2 2) Acenaphthylene 20.10 152 5302481 39.08 ug/1 100 2 3) Acenaphthene 20.67 153 3753726 38.70 ug/1 99 24) 2,4-Dinitrotoluene 21.34 165 1324209 39.20 ug/1 99 25) Diethylphthalate 22.10 149 4341766 41.73 ug/1 100 26) 4-Chiorophenyl-phenylether 22.21 204 1788802 39.38 ug/1 98 27) Fluorene 22.18 166 3904792 39.23 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.69 77 5454228 50.73 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS1126.M Thu Jan 31 16:23:33 2002 Page 1

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