GCMS reference results for sample AD29735, Dec 2001

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Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\209\DATA\DEC2101\REFE.D Vial: 16 Acq On : 22 Dec 2001 11:24 pm Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 29 11:59 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 818273 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3147977 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1552904 20.00 ug/1 -0.02 29) Phenanthrene-dlO 24.97 188 2133135 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1184379 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 775928 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.06 235 100994 4.31 ug/mL -0.01 Spiked Amount 5.000 Recovery = 86.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.42 74 65104 1.81 ug/1 91 3) bis(2-Chloroethyl)ether 11.10 93 165116 2.92 ug/1 99 4) 1,3-Dichlorobenzene 11.58 146 100159 1.68 ug/1 96 5) 1,4-Dichlorobenzene 11.58 146 100159 1.66 ug/1 95 6) 1,2-Dichlorobenzene 12.23 146 114086 2.06 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 12.57 45 280444 3.90 ug/1 # 93 8) N-Nitroso-di-n-propylamine 12.96 70 112306 3.49 ug/1 97 9) Hexachloroethane 13.06 117 27582 1.26 ug/1 94 11) Nitrobenzene 13.37 77 144915 2.95 ug/1 99 12) 1sophorone 14.00 82 316715 3.35 ug/1 100 13) bis(2-Chloroethoxy)methane 14.70 93 185974 2.93 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 96723 2.12 ug/1 96 15) Naphthalene 15.33 128 422897 2.81 ug/1 99 16) Hexachlorobutadiene 15.88 225 24577 1.10 ug/1 96 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.84 162 225396 2.54 ug/1 99 20) Dimethylphthalate 19.94 163 312835 3.03 ug/1 100 21) 2,6-Dinitrotoluene 20.15 165 46411 1.90 ug/1 97 22) Acenaphthylene 20.09 152 343474 2.76 ug/1 99 23) Acenaphthene 20.64 153 265385 2.98 ug/1 98 24) 2,4-Dinitrotoluene 21.34 165 46931 1.51 ug/1 98 25) Diethylphthalate 22.06 149 324998 3.40 ug/1 99 26) 4-Chlorophenyl-phenylether 22.20 204 125504 3.01 ug/1 98 27) Fluorene 22.16 166 271923 2.98 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 305897 3.10 ug/L 99

(#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Tue Jan 29 12:04:23 2002 Page 1

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