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GCMS calibration table for TCLP method, Dec 2001

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Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.

NYC-WTC_000036947–000036949

Folder label: “GCMS X 12/7/01 A 12/18/01”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File M:\INSTRU~1\2O9\DATA\DEC13O1\CAL25.D Vial: 2 Acq On 13 Dec 2001 9:50 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 14:37 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.60 168 1081863 25.02 ug/1 # 93 31) 4-Bromophenyl-phenylether 23.66 248 603449 25.19 ug/1 97 32) Hexachlorobenzene 24.08 284 700107 26.57 ug/1 100 3 3) Phenanthrene 25.05 178 3221195 24.97 ug/1 99 3 4) Anthracene 25.18 178 3240263 25.20 ug/1 99 35) Di-n-butylphthalate 26.99 149 4307410 25.10 ug/1 99 3 6) Fluoranthene 28.66 202 3170363 25.46 ug/1 97 39) Pyrene 29.33 202 3253425 23.55 ug/1 98 40) Butylbenzylphthalate 31.50 149 1655205 22.94 ug/1 92 41) Benzo(a)anthracene 32.97 228 2324943 24.38 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 2184959 22.41 ug/1 99 43) Chrysene 33.10 228 2313358 24.74 ug/1 99 45) Di-n-Octylphthalate 35.03 149 3205469 21.42 ug/1 # 94 46) Benzo(b)fluoranthene 36.04 252 2088148 24.65 ug/1 98 47) Benzo(k)fluoranthene 36.11 252 2237086 25.73 ug/1 100 4 8) Benzo(a)pyrene 36.93 252 1800460 24.45 ug/1 99 4 9) Indeno(1,2,3-cd)pyrene 40.79 276 1659551 22.53 ug/1 97 50) Dibenz(a,h)anthracene 40.84 278 1307628 22.67 ug/1 98 51) Benzo(g,h,i)perylene 41.88 276 1357309 21.57 ug/1 94

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Thu Jan 10 12:45:37 2002 Page 2

NYC-WTC_000036948

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GCMS calibration table data, Nov 2001 · Box DEP Box 21

NYC-WTC_000033723

Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.

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