Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
NYC-WTC_000036947–000036949Folder label: “GCMS X 12/7/01 A 12/18/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File M:\INSTRU~1\2O9\DATA\DEC13O1\CAL25.D Vial: 2 Acq On 13 Dec 2001 9:50 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 14:37 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.60 168 1081863 25.02 ug/1 # 93 31) 4-Bromophenyl-phenylether 23.66 248 603449 25.19 ug/1 97 32) Hexachlorobenzene 24.08 284 700107 26.57 ug/1 100 3 3) Phenanthrene 25.05 178 3221195 24.97 ug/1 99 3 4) Anthracene 25.18 178 3240263 25.20 ug/1 99 35) Di-n-butylphthalate 26.99 149 4307410 25.10 ug/1 99 3 6) Fluoranthene 28.66 202 3170363 25.46 ug/1 97 39) Pyrene 29.33 202 3253425 23.55 ug/1 98 40) Butylbenzylphthalate 31.50 149 1655205 22.94 ug/1 92 41) Benzo(a)anthracene 32.97 228 2324943 24.38 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 2184959 22.41 ug/1 99 43) Chrysene 33.10 228 2313358 24.74 ug/1 99 45) Di-n-Octylphthalate 35.03 149 3205469 21.42 ug/1 # 94 46) Benzo(b)fluoranthene 36.04 252 2088148 24.65 ug/1 98 47) Benzo(k)fluoranthene 36.11 252 2237086 25.73 ug/1 100 4 8) Benzo(a)pyrene 36.93 252 1800460 24.45 ug/1 99 4 9) Indeno(1,2,3-cd)pyrene 40.79 276 1659551 22.53 ug/1 97 50) Dibenz(a,h)anthracene 40.84 278 1307628 22.67 ug/1 98 51) Benzo(g,h,i)perylene 41.88 276 1357309 21.57 ug/1 94
(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Thu Jan 10 12:45:37 2002 Page 2
NYC-WTC_000036948
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NYC-WTC_000036941
Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
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Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
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Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037375
Calibration records for gas chromatography mass spectrometry analysis of volatile organic compounds in environmental samples.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018799
Calibration report listing response factors and concentrations for multiple organic compounds analyzed on December 22, 2001.
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Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
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Laboratory report listing quantitative results and detection limits for various organic compounds in a GCMS reference sample analyzed on November 28, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016065
Calibration report showing retention times and response factors for deuterated internal standards used in PAH analysis.
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Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
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Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.
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Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
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NYC-WTC_000036944
Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
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