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GCMS calibration results for volatile organics, Dec 2001

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Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.

NYC-WTC_000017122–000017125

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) Data File : M:\INSTRU~1\209\DATA\DEC2701\CAL100A.D Vial: 2 Acq On : 28 Dec 2001 10:29 am Operator: 209 GALOS Sample : Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 15:09 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator! Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126 Compound R.T. Qlon Response Conc Unit Qvalue 30) N-Nitrosodiphenylamine 22.67 168 4355535 90.70 ug/l # 68 31) 4-Bromophenyl-phenylether 23.69 248 2444995 91.89 ug/1 93 32) Hexachlorobenzene 24.12 284 2697562 92.20 ug/l 94 33) Phenanthrene 25.10 178 12836293 89.61 ug/1 98 34) Anthracene 25.23 178 12722623 89.10 ug/l 99 35) Di-n-butylphthalate 27.03 149 17246987 90.48 ug/l # 98 36) Fluoranthene 28.71 202 13328580 96.39 ug/1 98 39) Pyrene 29.38 202 13502293 87.35 ug/l 99 40) Butylbenzylphthalate 31.53 149 7440895 92.17 ug/l # 87 41) Benzo(a) anthracene 33.02 228 10121118 94.86 ug/l 99 42) Bis(2-ethylhexyl)phthalate 33.32 149 9116677 83.57 ug/1 98 43) Chrysene 33.16 228 9627723 92.01 ug/l 98 45) Di-n-Octylphthalate 35.08 149 14481862 91.99 ug/l # 95 46) Benzo(b) fluoranthene 36.10 252 9135545 102.50 ug/l 99 47) Benzo(k) fluoranthene 36.10 252 9929131 108.54 ug/l 99 48) Benzo(a) pyrene 37.00 252 7845786 101.25 ug/l 99 49) Indeno(1,2,3-cd) pyrene 40.90 276 7685449m 99.18 ug/l 50) Dibenz(a,h) anthracene 40.97 278 6008653 99.02 ug/l 97 51) Benzo(g,h,i)perylene 42.03 276 6244571m 94.31 ug/l (#) = qualifier out of range (m) = manual integration CAL100A.D GCMS1126.M Thu Jan 10 11:50:50 2002 Page 2 NYC-WTC_000017124

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NYC-WTC_000017124Source: NYC Law Department, mirrored locally

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