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GCMS reference analysis results for sample AD30643, Feb 2002

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Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018440–000018444

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\209\DATA\DEC2701\REFE.D Vial: 52 Acq On : 30 Dec 2001 9:15 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 31 16:14 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update * : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.61 168 113674 1.95 ug/1 98 31) 4-Bromophenyl-phenylether 23.66 248 77417 2.40 ug/1 97 32) Hexachlorobenzene 24.08 284 86678 2.44 ug/1 97 3 3) Phenanthrene 25.05 178 450477 2.59 ug/1 100 3 4) Anthracene 25.18 178 401592 2.32 ug/1 98 35) Di-n-butylphthalate 27.00 149 575477 2.49 ug/1 99 36) Fluoranthene 28.67 202 425359 2.53 ug/1 98 39) Pyrene 29.34 202 433022 2.39 ug/1 98 40) Butylbenzylphthalate 31.50 149 168001 1.77 ug/1 96 41) Benzo(a)anthracene 32.97 228 283001 2.26 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 253487 1.98 ug/1 98 43) Chrysene 33.09 228 329393 2.68 ug/1 99 45) Di-n-Octylphthalate 35.04 149 205834 1.24 ug/1 95 46) Benzo(b)fluoranthene 36.06 252 217152 2.31 ug/1 98 47) Benzo(k)fluoranthene 36.11 252 285049 2.96 ug/1 98 48) Benzo(a)pyrene 36.95 252 151439 1.85 ug'/l 98 49) Indeno(1,2,3-cd)pyrene 40.85 276 129610 1.59 ug/1 96 5 0) Dibenz(a,h)anthracene 40.91 278 110336 1.72 ug/1 97 51) Benzo(g,h,i)perylene 41.93 276 124764 1.79 ug/1 95

(#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Thu Jan 31 16:17:40 2002 Page 2

NYC-WTC_0000 18443

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NYC-WTC_000018443Source: NYC Law Department, mirrored locally

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