Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
NYC-WTC_000036941–000036943Folder label: “GCMS X 12/7/01 A 12/18/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : M:\INSTRU~1\2O9\DATA\DEC13O1\REFA.D Vial: 17 Acq On : 14 Dec 2001 12:31 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 1:19 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.60 168 148079 2.40 ug/1 94 31) 4-Bromophenyl-phenylether 23.66 248 83566 2.44 ug/1 98 32) Hexachlorobenzene 24.07 284 89374 2.38 ug/1 99 3 3) Phenanthrene 25.04 178 485679 2.64 ug/1 99 3 4) Anthracene 25.17 178 439006 2.39 ug/1 99 35) Di-n-butylphthalate 26.98 149 681596 2.78 ug/1 99 36) Fluoranthene 28.65 202 467049 2.63 ug/1 100 39) Pyrene 29.32 202 485769 2.45 ug/1 99 40) Butylbenzylphthalate 31.49 149 210274 2.03 ug/1 89 41) Benzo(a)anthracene 32.96 228 354052 2.59 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 291053 2.08 ug/1 99 43) Chrysene 33.08 228 397128 2.96 ug/1 99 45) Di-n-Octylphthalate 35.03 149 321161 1.53 ug/1 # 92 46) Benzo(b)fluoranthene 36.04 252 264675 2.22 ug/1 99 47) Benzo(k)fluoranthene 36.09 252 357837 2.93 ug/1 98 4 8) Benzo(a)pyrene 36.93 252 220377 2.13 ug/1 97 49) Indeno(l,2,3-cd)pyrene 40.77 276 213128 2.06 ug/1 95 5 0) Dibenz(a,h)anthracene 40.84 278 176853 2.18 ug/1 96 51) Benzo(g,h,i)perylene 41.86 276 186896 2.11 ug/1 # 89
(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Thu Jan 10 12:42:25 2002 Page 2
NYC-WTC_000036942
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NYC-WTC_000036947
Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
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Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.
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Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
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Gas chromatography-mass spectrometry calibration analysis documenting retention times and response values for deuterated reference standards from January 25, 2002.
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Instrument data file from February 2002 listing retention times and concentrations for polycyclic aromatic hydrocarbon surrogates.
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