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GCMS calibration results for sample AD29735, Dec 2001

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Calibration report listing response factors and concentrations for multiple organic compounds analyzed on December 22, 2001.

NYC-WTC_000018799–000018802

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File M: \ INSTRU-1 \2 0 9\DATA\DEC2101 \ CAL4 0A. D Vial: 2 Acq On 22 Dec 2001 7:50 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINTP Quant Time: Jan 29 12:11 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.63 168 2990511 38.01 ug/1 91 31) 4-Bromophenyl-phenylether 23.68 248 1661974 38.13 ug/1 92 32) Hexachlorobenzene 24.10 284 1867687 38.96 ug/1 94 3 3) Phenanthrene 25.07 178 8813147 37.55 ug/1 100 34) Anthracene 25.21 178 8473851 36.23 ug/1 99 35) Di-n-butylphthalate 27.01 149 11935896 38.22 ug/1 99 36) Fluoranthene 28.68 202 9057241 39.98 ug/1 98 3 9) Pyrene 29.35 202 9226131 34.78 ug/1 98 40) Butylbenzylphthalate 31.52 149 4911779 35.45 ug/1 94 41) Benzo(a)anthracene 32.99 228 6878692 37.57 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.30 149 6264424 33.46 ug/1 97 43) Chrysene 33.12 228 6657072 37.07 ug/1 100 45) Di-n-Octylphthalate 35.05 149 9882048 36.71 ug/1 96 46) Benzo(b)fluoranthene 36.07 252 5995090 39.33 ug/1 98 47) Benzo(k)fluoranthene 36.07 252 6455389m 41.27 ug/1 48) Benzo(a)pyrene 36.97 252 5084451 38.37 ug/1 99 49) Indeno (1,2,3-cd) pyrene 40.84 276 5152212 38.88 ug/1 98 50) Dibenz(a,h)anthracene 40.90 278 4075014 39.27 ug/1 99 51) Benzo(g,h,i)perylene 41.95 276 4156522 36.71 ug/1 98

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS1126.M Tue Jan 29 12:14:56 2002 Page 2

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NYC-WTC_000018801Source: NYC Law Department, mirrored locally

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