GCMS calibration results for volatile organics, Dec 2001

NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) Data File : M:\INSTRU~1\209\DATA\DEC2701\CAL100A.D Vial: 2 Acq On : 28 Dec 2001 10:29 am Operator: 209 GALOS Sample : Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 15:09 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator] Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min 1) 1,4-Dichlorobenzene-d4 11.69 152 934272 20.00 ug/l 0.00 10) Naphthalene-de 15.30 136 3650231 20.00 ug/l 0.00 17) Acenaphthene-d10 20.57 164 1772172 20.00 ug/l 0.00 29) Phenanthrene-d10 25.01 188 2704802 20.00 ug/l 0.01 38) Chrysene-d12 33.06 240 1790805 20.00 ug/l 0.02 44) Perylene-d12 37.14 264 1184795 20.00 ug/1 0.02 System Monitoring Compounds 37) 2,4-DDD 0.00 235 od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.48 74 5042881 gags ug/1 82 3) bis (2-Chloroethyl) ether 11.15 93 6922506 07.34 ug/l 94 4) 1,3-Dichlorobenzene 11.59 146 6470259 95.23 ug/1 99 5) 1,4-Dichlorobenzene 11.74 146 6354926 92.49 ug/1 98 6) 1,2-Dichlorobenzene 12.25 146 5776862 91.17 ug/l 98 7) 2,2'-oxybis(1-Chloropropan 12.59 45 9849713 119.93 ug/1 95 8) N-Nitroso-di-n-propylamine 13.03 70 4352784 118.47 ug/l 92 9) Hexachloroethane 13.08 117 2599778 04.93 ug/l 93 11) Nitrobenzene 13.40 77 6988921 Gate ug/1 90 12) Isophorone 14.07 82 13058986 +14 ug/l 94 13) bis(2-Chloroethoxy)methane 14.73 93 8009398 108.77 ug/l 99 14) 1,2,4-Trichlorobenzene 15.20 180 4885084 92.16 ug/l 99 15) Naphthalene 15.38 128 15654386 89.75 ug/l 99 16) Hexachlorobutadiene 15.90 225 2408977 93.26 ug/l 100 18) Hexachlorocyclopentadiene 18.07 237 1513703 118.56 ug/1 98 19) 2-Chloronaphthalene 18.86 162 9225430 91.25 ug/l 94 20) Dimethylphthalate 20.00 163 11390340 96.71 ug/l 100 21) 2,6-Dinitrotoluene 20.21 165 2868852 103.09 ug/l # 61 22) Acenaphthylene 20.12 152 13160477 92.62 ug/1 100 23) Acenaphthene 20.70 153 9042964 89.01 ug/l 99 24) 2,4-Dinitrotoluene 21.39 165 3777081 106.76 ug/l # 79 25) Diethylphthalate 22.14 149 10777314 98.89 ug/1 98 26) 4-Chlorophenyl-phenylether 22.24 204 3758471 00 ug/l 93 27) Fluorene 22.21 166 8287522 79449 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.72 77 12985351 5.32 ug/L # 90 (#) = qualifier out of range (m) = manual integration CAL100A.D GCMS1126.M Thu Jan 10 11:50:45 2002 Page 1 NYC-WTC_000017123