GCMS blank analysis results for sample AD28143, Nov 2001

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\209\DATA\NOV2601\REF.D Vial: 22 Acq On : 27 Nov 2001 7:14 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 13:11 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcqMeth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.69 152 737564 20.00 ug/1 0.00 10) Naphthalene-d8 15.30 136 2771521 20.00 ug/1 0.00 17) Ac enapht hene-d10 20.57 164 1336543 20.00 ug/1 0.00 29) Phenanthrene-dlO 25.00 188 1803858 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 905649 20.00 ug/1 0.00 44) Perylene-dl2 37.11 264 597398 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 113805 5.74 ug/mL 0.00 Spiked Amount 5.000 Recovery = 114.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.44 74 69578 2.14 ug/1 94 3) bis(2-Chloroethyl)ether 11.12 93 182135 3.58 ug/1 99 4) 1,3-Dichlorobenzene 11.59 146 126156 2.35 ug/1 98 5) 1,4-Dichlorobenzene 11.59 146 126156 2.33 ug/1 98 6) 1,2-Dichlorobenzene 12.25 146 141571 2.83 ug/1 97 7) 2,21-oxybis(1-Chloropropan 12.59 45 256885 3.96 ug/1 94 8) N-Nitroso-di-n-propylamine 12.98 70 103184 3.56 ug/1 97 9) Hexachloroethane 13.08 117 35716 1.81 ug/1 85 11) Nitrobenzene 13.37 77 142327 3.29 ug/1 96 12) 1sophorone 14.02 82 315163 3.79 ug/1 97 13) bis(2-Chloroethoxy)methane 14.70 93 214430 3.84 ug/1 98 14) 1,2,4-Trichlorobenzene 15.19 180 116568 2.90 ug/1 99 15) Naphthalene 15.36 128 491752 3.71 ug/1 99 16) Hexachiorobutadiene 15.91 225 37162 1.89 ug/1 97 18) Hexachlorocyclopentadiene 18.08 237 2428 0.25 ug/1 # 79 19) 2-Chloronaphthalene 18.85 162 268953 3.53 ug/1 98 20) Dimethylphthalate 19.95 163 340499 3.83 ug/1 100 21) 2,6-Dinitrotoluene 20.16 165 53980m 2.57 ug/1 22) Acenaphthylene 20.10 152 399827 3.73 ug/1 100 2 3) Acenaphthene 20.66 153 300911 3.93 ug/1 100 24) 2,4-Dinitrotoluene 21.32 165 60808 2.28 ug/1 # 88 25) Diethylphthalate 22.08 149 325101 3.96 ug/1 99 26) 4-Chlorophenyl-phenylether 22.21 204 144366 4.02 ug/1 98 27) Fluorene 22.18 166 311453 3.96 ug/1 97 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 267122 3.15 ug/L 97

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Wed Jan 09 13:12:10 2002 Page 1

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