GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.
NYC-WTC_000036931–000036940Folder label: “GCMS X 12/7/01 A 12/18/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File M:\INSTRU~l\209\DATA\DEC1801\29565.D Vial: 3 Acq On 18 Dec 2001 6:01 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 11:39 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NP091101
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 798854 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3030603 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1528069 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2191297 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1440237 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 931541 20.00 ug/1 -0.01
System Monitoring Compounds 37) 2,4-DDD 30.06 235 131705 5.47 ug/mL -0.01 Spiked Amount 5.000 Recovery = 109.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 1548 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 13.50 82 193 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1099 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. .18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.18 165 186 N.D. 25) Diethylphthalate 22.10 149 368 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 29565.D. GCMS1126.M Thu Jan 10 12:36:44 2002 Page 1
NYC-WTC_000036933
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