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GCMS analysis results for sample AD29565, Jan 2002

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GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.

NYC-WTC_000036931–000036940

Folder label: “GCMS X 12/7/01 A 12/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File M:\INSTRU~l\209\DATA\DEC1801\29565.D Vial: 3 Acq On 18 Dec 2001 6:01 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 11:39 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via .: Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorpbenzene 0.00 284 0 N.D. 33) Phenanthrene 25.05 178 725 N.D. 34) Anthracene 25.05 178 725 N.D. 35) Di-n-butylphthalate 27.00 149 45438 0.29 ug/1 # 97 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.01 228 3988 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 5541 N.D. 43) Chrysene 33.09 228 595 N.D. 45) Di-n-Octylphthalate 34.99 149 1274 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.11 252 3778 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29565.D GCMS1126.M Thu Jan 10 12:36:49 2002 Page 2

NYC-WTC_000036934

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NYC-WTC_000036934Source: NYC Law Department, mirrored locally

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