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GCMS analysis results for sample AD28860, Dec 16 2001

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Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.

NYC-WTC_000018817–000018829

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : M:\lNSTRU~l\209\DATA\DEC2701\29735.D Vial: 18 Acq On : 29 Dec 2001 3:45 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 29 11:18 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.98 178 708 N.D. 3 4) Anthracene 24.98 178 708 N.D. 35) Di-n-butylphthalate 27.04 149 22784 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.03 228 4301 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 3998 N.D. 43) Chrysene 33.03 228 4301 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.13 252 3660 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29735.D GCMS1126.M Tue Jan 29 11:19:55 2002 Page 2

NYC-WTC_000018820

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NYC-WTC_000018820Source: NYC Law Department, mirrored locally

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