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GCMS analysis results for sample AD28861, Dec 17 2001

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GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.

NYC-WTC_000018849–000018857

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : M:\INSTRU~1\209\DATA\DEC2101\28861.D Vial: 18 Acq On : 23 Dec 2001 1:21 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 29 10:56 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.97 178 1593 N.D. 34) Anthracene 24.97 178 1593 N.D. 35) Di-n-butylphthalate 27.00 149 101505 0.47 ug/1 98 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 743 N.D. 41) Benzo(a)anthracene 33.01 228 4604 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 16166 N.D. 43) Chrysene 33.10 228 359 N.D. 45) Di-n-Octylphthalate 35.04 149 21,8 N.D. 46) Benzo(b)fluoranthene 36.17 252 190 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 P N.D. 4 8) Benzo(a)pyrene 37.12 252 4964 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28861.D GCMS1126.M Tue Jan 29 10:59:09 2002 Page 2

NYC-WTC_000018852

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NYC-WTC_000018852Source: NYC Law Department, mirrored locally

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