GCMS analysis results for sample AD28861, Dec 17 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\2O9\DATA\DEC21O1\28861.D Vial: 18 Acq On : 23 Dec 2001 1:21 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 29 10:56 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dich.lorobenzene-d4 11.67 152 1080356 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4144081 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.56 164 2094160 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3033179 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1866569 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 950124 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 162751 4.88 ug/mL -0.01 Spiked Amount 5.000 Recovery = 97.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 281 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 .0 N.D. 15) Naphthalene 15.34 128 1100 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.23 165 214 N.D. 25) Diethylphthalate 22.10 149 1223 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 28861.D GCMS1126.M Tue Jan 29 10:59:03 2002 Page 1

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