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GCMS results for unknowns, sample AD26827, Dec 2001

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GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.

NYC-WTC_000018898–000018912

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\209\DATA\DEC2701\26827.D Vial: 11 Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 29 11:21 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.98 178 1338 N.D. 3 4) Anthracene 24.98 178 1338 N.D. 35) Di-n-butylphthalate 27.01 149 72176 0.33 ug/1 99 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 29.44 202 266 N.D. 40) Butylbenzylphthalate 31.51 149 544 N.D. 41) Benzo(a)anthracene 33.02 228 5425 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 17799 N.D. 43) Chrysene 33.02 228 5425 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.13 252 5221 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 26827.D GCMS1126.M Tue Jan 29 11:22:40 2002 Page 2

NYC-WTC_000018901

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NYC-WTC_000018901Source: NYC Law Department, mirrored locally

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