NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : M:\lNSTRU~l\209\DATA\DEC2701\26827.D Vial: 11
Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 29 11:21 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Jan 25 15:57:52 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4 -Dichlorobenzene-d4 11.68 152 1048261 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 4056259 20.00 ug/1 -0.03
17) Acenaphthene-dlO 20.56 164 2050252 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.98 188 3103925 20.00 ug/1 -0.01
38) Chrysene-dl2 33.02 240 1937421 20.00 ug/1 -0.01
44) Perylene-dl2 37.12 264 1175695 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 199406 5.84 ug/mL -0.01
Spiked Amount 5.000 Recovery = 116.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bi s(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichiorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.33 128 1375 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.33 165 177 N.D.
25) Diethylphthalate 22.13 149 1583 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
26827.D GCMS1126.M Tue Jan 29 11:22:35 2002 Page 1
NYC-WTC_000018900
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