Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
NYC-WTC_000018287–000018315Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\ JANI 802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 1-Monolinoleoylglycerol trimet Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 34.19 1.41 ug/1 545671 Chrysene-dl2 32.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Trisiloxa ne, 1,1,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 38 4 Ethanedioic acid, bis (trimethylsily 234 C8H1804Si2 018294-04-7 32 Abundance / Scan 3175 (34.194 min): 30986A.D (-) m/ z 72.95 100.00% 73
5000 147 221 281 355 33.80 34.00 34.20 34.40 34.80 ; । m/z-> 45 50 100 117 ' 1 ri1T 174 I ■ ' 150 41914 200 r , j 249. 11 1* I “. j 327 Fi ri r |“ti 401449 ITim fr । r i t t । ri i i । । j 250 300 350 400 450 500 550 m/z 147.00 47.72% Abundance #58871:1-Monolinoteoylglycerol trimethylsilyl ether 73 207 5000 147 33.80 34.00 34.20 34.40 34.60 34 103 281 m/z 221.05 2 7.65%
miz-> 50 100 150 200 250 ’300 i .. 395 ,42 350 400 450 500 550 ’ Abundance #60503: 3-Isopropoxy-1,1.1,7.7.7-hexamethyl-3,5,5-tris(trim 73
33.80 34.00 3420 3440 3460 5000 m/z 281.00 15.76% 147
221 281 327 415 519 561 T i I j i m i } « > » j r Ai i । i 1g i 1T [ 1 r ।» » i I 1 i | m i I j r 1 i y t i Wz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet —In.—mBofrr 73 33.80 34.00 34.20 34.40 34.60 147 m/z 355.0 14.03% 5000 281 45 369
m/z-> ' > l’ 1 50 117 100 4, ,297, 249- i j i < 1*1 * it iji i । i 1* 1 1 । * > * > | I r 150 200 250 300 350 400 450 500 550 1**4411*1 1I9m r r 33.80 34.00 34.20 34.40 34.60
30986A.D GCMS1126.M Tue Jan 22 10:18:45 2002 Page 18
NYC-WTC_000018312
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder