GCMS blank analysis for sample AD30694, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\1\DATA\DEC3101\LBD.D vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method. : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Heptanol, 5-methyl- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

7.76 0.51 ug/1 155777 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Heptanol, 5-methyl- 130 C8H180 018720-65-5 36 2 1,8-Nonanediol, 8-methyl- 174 C10H22O2 054725-73-4 33 3 tert-Butyl Hydroperoxide 90 C4H10O2 000075-91-2 33 4 1-Butanol, 4-ethoxy- 118 C6H14O2 000111-73-9 28 Abundance Scan 296 (7.764 mtn): LBD.D (-) m/z 4 .05 100.00% 43 59

5000 101 118/8/3 i j j ift 11 i | 11s i 7.40 7.60 7.80 8.00 8.20

miz—> 20 —+++ 30> 40 36 i +50 50 60 70 70 80 90 84 • • । 1* । । 100 110 ।।. 120 130 m/z 59.05 78.86% Abundance #5541:3-Heptanol, 5-methyl- 59

83 5000 N 27 7.40 7.60 7.80 8.00 8.20 45 101 m/z 101.05 30.55% ■ i ' ■ ■ ■ i ‘ ■ i • ' I • ■ > I l l | i .........I.. ■ ..... . miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16264; 1,8-Nonanediol, 8-methyl- 59 I I TFT* I J 1 -r-r-pr 7.40 7.60 7.80 8.00 8.20 5000 m/ z 16.21%

42 69 83 98 123 TPBBBB—BTTT • i ■ ■ ' * i ■ ■ ‘ ■ i • 1 ■ ■ i ■ ■ • 1 i ■ ' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #922: tert-Butyl Hydroperoxide • i ■ ‘ • i ‘ ■ i 1 59 7.40 7.60 7.80 8.00 8.20 43 m/z 41.05 13.41% 5000

31 , 1 miz-> 111123711 20 30 40 ‘50‘ 6o ‘ ‘ 70 ’80 90 "100’110’ 120 130 STpn——mgn—mT-mCT 7.40 7.60 7.80 8.00 8.20

LBD.D GCMS1126.M Wed Jan 23 09:02:00 2002 Page 2

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