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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

30.25 1.48 ug/1 447203 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW Mol Form CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 4 Benzoic acid, 2,4-bis [ (trimethylsil 370 C16H30O4Si3 010586-16-0 16 Abundance Scan 2745 (30.246 min): LBD.D (-) m/z 72.9,5 100.00% 73

5000 147 221 ‘ r f ’* I 1i I l f l | < i . | . i 281 355 30.00 30.20 30.40 30.60 45 ” , 117 191 [ 249, 325, | 401 429 .......... . ’ i rI i r TdTRTTTT1tt—1ur’1————1T m/z 147.00 37.17% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 34 30.00 30.20 30.40 30.60 103 I 281 m/z 221.05 21.85% 395 I । । , 482 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714: 1.1,1.5,7.7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 • • i i • ■ i • 1 1 • i 1 • 147 30.00 30.20 30.40 30.60 5000 267 m/z 355.0 12.85% I 355 429 45 207

miz-> 50 i66 ‘ 150 ‘ 200 250 300 350 ‘ 400 450 500 550 (Abundance #60503:3-isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 30.00 30.20 30.40 30.60 m/z 281.00 12.69% 5000 147

2211________281I 327 i । 415 i 519 561 miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60

LBD.D GCMS1126.M Wed Jan 23 09:02:57 2002 Page 13

NYC-WTC_000018087

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NYC-WTC_000018087Source: NYC Law Department, mirrored locally

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