NYC 9/11 Public Portal Document
Quantitation Report (Not Reviewed)
' Data File C: \HPCHEM\ 1 \DATA\ JAN0 802\30903.D Vial: 23
Acq On 9 Jan 2002 11:46 am Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 9 14:40 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Jan 07 10:31:02 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.52 152 859077 20.00 ug/1 0.00
10) Naphthalene-d8 15.12 136 3279066 20.00 ug/1 0.00
17) Acenaphthene-diO 20.39 164 1609291 20.00 ug/1 0.00
2 9) Phenanthrene -dl0 24.81 188 2398149 20.00 ug/1 0.00
38) Chrysene-dl2 32.84 240 1437420 20.00 ug/1 0.00
44) Perylene-dl2 36.91 264 833660 20.00 ug/1 0.01
System Monitoring Compounds
37) 2,4-DDD 29.88 235 109742 3.99 ug/mL -0.19
Spiked Amount 5.000 Recovery = 79.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D. '
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4 -Tri chlorobenzene' 0.00 180 0 N.D.
15) Naphthalene 15.18 128 880 N.D.
16) Hexachiorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
2 2) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.86 165 1537 N.D.
25) Diethylphthalate 21.92 149 841 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30903.D GCMS1126.M Wed Jan 09 14:44:07 2002 Page 1
NYC-WTC_000017573
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