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GCMS analysis report for sample AD31021, Jan 2002

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Laboratory record of GCMS analysis for unknown compounds in sample AD31021 conducted on January 18, 2002.

NYC-WTC_000017585–000017594

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document a Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\JANO802\31021.D Vial: 22 Acq On : 9 Jan 2002 10:47 am Operator: 209 GALOS Sample + gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 14:39 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 827822 20.00 ug/1 0.00 10) Naphthalene-ds 15.13 136 3179494 20.00 ug/1 0.00 17) Acenaphthene-d1o 20.39 164 1554828 20.00 ug/l 0.00 29) Phenanthrene-d10 24.80 188 2311003 20.00 ug/1 0.00. 38) Chrysene-di12 32.84 240 1379556 20.00 ug/l 0.00 44) Perylene-d12 36.90 264 797689 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 29.89 235 117990 4.45 ug/mL -0.18 Spiked Amount 5.000 Recovery = 89.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. * 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. > 5) 1,4-Dichlorobenzene 0.00 146 0) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 0.00 77 ° N.D. 12) Isophorone 14.05 82 * 283 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 ° N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.19 128 593 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 0.00 162 ° N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. a 22) Acenaphthylene 0.00 152 ° N.D. 23) Acenaphthene 0.00 153 0 N.D. . 24) 2,4-Dinitrotoluene 20.65 165 671 N.D. 25) Diethylphthalate 21.91 149 374 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 ° N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 31021.D GCMS1126.M Wed Jan 09 14:43:33 2002 Page 1 NYC-WTC_000017587

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