GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02”

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NYC 9/11 Public Portal Document a Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\JAN0802\31019.D Vial: 24 Acq On : 9 Jan 2002 12:45 pm Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 14:40 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 920374 20.00 ug/l 0.00 10) Naphthalene-ds 15.12 136 3524055 20.00 ug/l 0.00 17) Acenaphthene-d10 20.39 164 1744331 20.00 ug/l 0.00 29) Phenanthrene-d10 24.81 188 2594681 20.00 ug/1 0.00 38) Chrysene-d12 32.84 240 1626983 20.00 ug/l 0.00 44) Perylene-d12 36.91 264 948029 20.00 ug/l 0.01 System Monitoring Compounds 37) 2,4-DDD 29.89 235 155427 5.22 ug/mL -0.18 Spiked Amount 5.000 Recovery = 104.40% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 182 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 ° N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5 5) 1,4-Dichlorobenzene 0.00 146 ° N.D. 6) 1,2-Dichlorobenzene 0.00 146 ° N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 0) N.D. 11) Nitrobenzene 0.00 «77 0) N.D. 12) Isophorone 0.00 82 0) N.D. + 13) bis(2-Chloroethoxy)methane 0.00 93 o N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ce) N.D. 15) Naphthalene 15.18 128 820 N.D. 16) Hexachlorobutadiene 0.00 225 0) N.D. 18) Hexachlorocyclopentadiene 0.00 237 0) N.D. 19) 2-Chloronaphthalene 18.21 162 250 N.D. 20) Dimethylphthalate 20.12 163 370 N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° _N.D. a 22) Acenaphthylene 20.06 152 192 N.D. 23) Acenaphthene 0.00 153 ° N.D. . 24) 2,4-Dinitrotoluene 20.85 165 1959 N.D. 25) Diethylphthalate 21.92 149 621 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 ) N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 te) N.D. (#) = qualifier out of range (m) = manual integration 31019.D GCMS0103.M Thu Jan 10 08:43:12 2002 Page 1 NYC-WTC_000017557

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NYC-WTC_000017557Source: NYC Law Department, mirrored locally

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