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GCMS analysis results for sample AD30631, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30631 conducted on January 22, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017290–000017298

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN0302\30631.D 1 V Vial: 30 Acq On : 4 Jan 2002 2:46 pm Operator: 209 GALOS Sample : gems scan 1/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 15:35 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.53 152 652724 20.00 ug/1 -0.17 10) Naphthalene-d8 15.12 136 2555253 20.00 ug/1 -0.19 17) Acenaphthene-diO 20.39 164 1278051 20.00 ug/1 -0.19 29) Phenanthrene-diO 24.81 188 1763157 20.00 ug/1 -0.19 38) Chrysene-dl2 32.83 240 983807 20.00 ug/1 -0.20 44) Perylene-dl2 36.90 264 560709 20.00 ug/1 -0.22

System Monitoring Compounds 37) 2,4-DDD 29.88 235 78443 4.05 ug/mL -0.19 Spiked Amount 5.000 Recovery = 81.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.11 74 104 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene .0.00 180 0 N.D. 15) Naphthalene 15.18 128 991 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.70 165 363 N.D. 25) Diethylphthalate 21.92 149 511 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30631.D GCMS0103.M Thu Jan 10 12:18:23 2002 Page 1

NYC-WTC_000017292

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NYC-WTC_000017292Source: NYC Law Department, mirrored locally

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