NYC 9/11 Public Portal Document
Quantitation Report Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN0302\29519.D Vial: 22
Acq On : 4 Jan 2002 7:00 am Operator: 209 GALOS
Sample : gems scan 1/2 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 4 7:49 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via,: Initial Calibration
DataAcq Meth': GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 659542 20.00 ug/1 -0.17
10) Naphthalene-d8 15.12 136 2570005 20.00 ug/1 -0.19
17) Acenaphthene-diO 20.39 164 1290434 20.00 ug/1 -0.19
2 9) Phenanthrene-dl0 24.80 188 1813895 20.00 ug/1 -0.19
38) Chrysene-dl2 32.83 240 1103583 20.00 ug/1 -0.21
44) Perylene-d12 36.89 264 656207 20.00 ug/1 -0.22
System Monitoring Compounds
37) 2,4-DDD 29.88 235 97986 4.91 ug/mL -0.19
Spiked Amount 5.000 Recovery = 98.20%
Target Compounds Qvalue
2) N- nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’ -oxybis(1-chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.18 128 1974 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.75 165 272 N.D.
25) Diethylphthalate 21.91 149 628 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29519.D GCMS0103.M Thu Jan 10 12:14:03 2002 Page 1
NYC-WTC_000049863
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