NYC 9/11 Public Portal Document
Quantitation Report Reviewed)
Data File C:\HPCHEM\l\DATA\JAN0302\29562.D Vial: 21
Acq On 4 Jan 2002 6:02 am Operator: 209 GALOS
Sample gems scan 1/2 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 4 6:51 2002 Quant Results File: GCMS1126.RES
Quant Method. : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.52 152 655438 20.00 ug/1 -0.18
10) Naphthalene-d8 15.12 136 2548702 20.00 ug/1 -0.19
17) Acenaphthene-dl0 20.39 164 1275695 20.00 ug/1 -0.19
29) Phenanthrene-diO 24.81 188 1784822 20.00 ug/1 -0.19
38) Chrysene-dl2 32.83 240 1026016 20.00 ug/1 -0.20
44) Perylene-dl2 36.90 264 594393 20.00 ug/1 -0.22
System Monitoring Compounds
37) 2,4-DDD 29.88 235 88928 4.53 ug/mL -0.19
Spiked Amount 5.000 Recovery = 90.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’ -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.19 128 1452 N.D.
16) Hexachiorobutadiene 0.00 225 0 N.D.
18) Hexachiorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.74 165 283 N.D.
25) Diethylphthalate 21.91 149 423 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29562.D GCMS0103.M Thu Jan 10 12:13:31 2002 Page 1
NYC-WTC_000049872
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