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GCMS analysis log for sample AD30632

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30632 on January 22, 2002.

NYC-WTC_000017320–000017328

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017322
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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) . Data File : C:\HPCHEM\1\DATA\JAN0302\30632.D Vial: 27 Acq On : 4 dan 2002 11:51 am Operator: 209 GALOS Sample : gems scan 1/2 Inst : GC/MS 209 Misc 3 Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 12:39 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.52 152 618530 20.00 ug/l -0.18 10) Naphthalene-de 15.12 136 2452798 20.00 ug/l -0.18 17) Acenaphthene-d10 20.39 164 1236829 20.00 ug/l -0.18 29) Phenanthrene-d10 24.81 188 1690288 20.00 ug/l -0.18 38) Chrysene-d12 32.83 240 914518 20.00 ug/l -0.20 44) Perylene-di2 36.90 264 518801 20.00 ug/l -0.22 System Monitoring Compounds 37) 2,4-DDD 29.88 235 83616 4.50 ug/ml -0.19 Spiked Amount 5.000 Recovery = 90.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0) N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 ° N.D. 6) 1,2-Dichlorobenzene 0.00 146 ° N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 «77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0) N.D. 15) Naphthalene 15.18 128 4109 N.D. 16) Hexachlorobutadiene 0.00 225 ° N.D. 18) Hexachlorocyclopentadiene 0.00 237 ) N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 ) N.D. 23) Acenaphthene 0.00 153 0) N.D. 24) 2,4-Dinitrotoluene 20.71 165 289 N.D. 25) Diethylphthalate 21.92 149 664 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 oO N.D. (#) = qualifier out of range (m) = manual integration 30632.D GCMS1126.M Tue Jan 15 09:46:44 2002 Page 1 NYC-WTC_000017322

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NYC-WTC_000017322Source: NYC Law Department, mirrored locally

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