NYC 9/11 Public Portal Document
Quantitation Report eviewed)
Data File C:\HPCHEM\1\DATA\JAN03 02\2 92 84.D Vial: 24
Acq On 4 Jan 2002 8:56 am Operator: 209 GALOS
Sample gems scan 1/2 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 4 9:45 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update ’ : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. QIon Response Cone Units Dev (Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 665626 20.00 ug/1 -0.17
10) Naphthalene-d8 15.12 136 2611111 20.00 ug/1 -0.19
17) Acenaphthene-dl0 20.39 164 1324591 20.00 ug/1 -0.19
29) Phenanthrene-diO 24.80 188 1831142 20.00 ug/1 -0.19
38) Chrysene-dl2 32.84 240 1005529 20.00 ug/1 -0.20
44) Perylene-dl2 36.90 264 588697 20.00 ug/1 -0.22
System Monitoring Compounds
37) 2,4-DDD 29.88 235 94603 4.70 ug/mL -0.19
Spiked Amount 5.000 Recovery = 94.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 13.91 82 221 N.D.
13) bis(2-Chloroethoxy)methane 14.59 93 195 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.18 128 1835 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachiorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 19.79 163 625 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 19.95 152 489 N.D.
23) Acenaphthene 20.48 153 451 N.D.
24) 2,4-Dinitrotoluene 20.68 165 358 N.D.
25) Diethylphthalate 21.91 149 4275 N.D.
26) 4-Chlorophenyl-phenylether 22.04 204 383 N.D.
27) Fluorene 22.01 166 635 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29284.D GCMS0103.M Thu Jan 10 12:15:07 2002 Page 1
NYC-WTC_000049807
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