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GCMS analysis results, sample AD29284, January 2002

Machine-extracted title · confidence 70%

Gas chromatography-mass spectrometry analysis report for sample AD29284 showing surrogate compound recovery at 94 percent and unknown compound detection.

NYC-WTC_000049805–000049813

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN0302\29284.D Vial: 24 Acq On : 4 Jan 2002 8:56 am Operator: 209 GALOS Sample : gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 9:45 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title . : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.87 178 1387 N.D. 3 4) Anthracene 25.00 178 862 N.D. 35) Di-n-butylphthalate 26.83 149 8113 N.D. 3 6) Fluoranthene 28.50 202 1070 N.D. 39) Pyrene 29.16 202 1181 N.D. 40) Butylbenzylphthalate 31.32 149 208 N.D. 41) Benzo(a)anthracene 32.83 228 3114 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 7452 N.D. 43) Chrysene 32.92 228 862 N.D. 45) Di-n-Octylphthalate 34.87 149 501 N.D. 46) Benzo(b)fluoranthene 35.87 252 924 N.D. 47) Benzo(k)fluoranthene 35.87 252 1043 N.D. 4 8) Benzo(a)pyrene 36.75 252 1170 N.D. . 49) Indeno(l,2,3-cd)pyrene 40.52 276 1922 N.D. 50) Dibenz(a,h)anthracene 40.63 278 419 N.D. 51) Benzo(g,h,i)perylene 41.56 276 2629 N.D.

(#) = qualifier out of range (m) = manual integration 29284.D GCMS0103.M Thu Jan 10 12:15:11 2002 Page 2

NYC-WTC_000049808

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NYC-WTC_000049808Source: NYC Law Department, mirrored locally

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