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GCMS analysis results for sample AD29519, Jan 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD29519 including unknown compounds and surrogate recovery data.

NYC-WTC_000049851–000049860

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\JAN0302\29465.D Vial: 28 Acq On : 4 Jan 2002 12:49 pm Operator: 209 GALOS Sample : gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 13:38 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue • 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.88 178 110 N.D. 34) Anthracene 24.88 178 110 N.D. 35) Di-n-butylphthalate 26.84 149 6417 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.83 228 2458 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 13411 N.D. 43) Chrysene 32.83 228 2458 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.89 252 2396 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29465.D GCMS0103.M Thu Jan 10 12:17:22 2002 Page 2

NYC-WTC_000049854

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NYC-WTC_000049854Source: NYC Law Department, mirrored locally

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