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GCMS blank analysis results for sample AD29228, January 2002

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Blank analysis report for GCMS testing of sample AD29228 conducted on January 10, 2002.

NYC-WTC_000049795–000049804

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\JAN0302\29228.D Vial: 20 Acq On : 4 Jan 2002 5:04 am Operator: 209 GALOS Sample : gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 5:53 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.88 178 230 N.D. 34) Anthracene 24.88 178 230 N.D. 35) Di-n-butylphthalate 26.83 149 3434 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 4 0) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.83 228 3350 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 1359 N.D. 43) Chrysene 32.91 228 356 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 35.88 252 1423 N.D. 47) Benzo(k)fluoranthene 35.94 252 749 N.D. 48) Benzo(a)pyrene 36.74 252 237 N.D. 49) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g,h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29228.D GCMS0103.M Thu Jan 10 12:13:01 2002 Page 2

NYC-WTC_000049798

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NYC-WTC_000049798Source: NYC Law Department, mirrored locally

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