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GCMS analysis results for sample AD30631, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30631 conducted on January 22, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017290–000017298

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File C: \HPCHEM\ 1 \DATA\ JAN0 302\30631.D Vial: 30 Acq On 4 Jan 2002 2:46 pm Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 15:35 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.81 178 576 N.D. 3 4) Anthracene 24.81 178 576 N.D. 35) Di-n-butylphthalate 26.83 149 2245 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.83 228 2360 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 917 N.D. 43) Chrysene 32.83 228 2360 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.90 252 2195 N.D. 49) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30631.D GCMS0103.M Thu Jan 10 12:18:26 2002 Page 2

NYC-WTC_000017293

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NYC-WTC_000017293Source: NYC Law Department, mirrored locally

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