GCMS reference scan results

NYC 9/11 Public Portal Document fo Quantitation Report (QT Reviewed . Data File : C:\HPCHEM\1\DATA\JAN0802\REFB.D Vial: 19 Acq On : 9 dan 2002 6:53 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 7:42 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. QIon Response Conc Units Dev (Min! 1) 1,4-Dichlorobenzene-d4 11.52 152 777743 20.00 ug/1 0.00 10) Naphthalene-ds 15.12 136 2985890 20.00 ug/1 0.00 17) Acenaphthene-d10 20.39 164 1455111 20.00 ug/l 0.00 29) Phenanthrdne-d10 24.81 188 2167715 20.00 ug/1 0.00 38) Chrysene-d12 32.84 240 1326180 20.00 ug/l 0.00 44) Perylene-di2 36.90 264 785434 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 29.88 235 117428 4.72 ug/ml -0.19 Spiked Amount 5.000 Recovery = 94.40% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 73193 1.96 ug/l 96 3) bis(2-Chloroethyl) ether 10.96 93 184810 3.07 ug/1 97 4) 1,3-Dichlorobenzene 11.43 146 124750 2.32 ug/1 97 5) 1,4-Dichlorobenzene 11.43 146 124750 2.30 ug/1 97 6) 1,2-Dichlorobenzene 12.08 146 136218 2.72 ug/l 98 7) 2,2'-oxybis(1-Chloropropan 12.42 45 318332 3.55 ug/l 96 8) N-Nitroso-di-n-propylamine 12.81 70 126055 3.35 ug/1 97 9) Hexachloroethane 12.91 117 41184 1.86 ug/l 96 11) Nitrobenzene 13.20 77 173992 3.02 ug/l 97 12) Isophorone 13.85 82 372439 3.62 ug/l 98 13) bis(2-Chloroethoxy)methane 14.54 93 231640 3.48 ug/L 100 14) 1,2,4-Trichlorobenzene 15.02 180 110731 2.72 ug/1 99 15) Naphthalene 15.18 128 467517 3.42 ug/l] 100 16) Hexachlorobutadiene 15.73 225 38738 1.88 ug/1 97 18) Hexachlorocyclopentadiene- 17.91 237 932 N.D. 19) 2-Chloronaphthalene 18.67 162 257740 3.42 ug/1 98 20) Dimethylphthalate 19.78 163 349670 3.96 ug/l 100 21) 2,6-Dinitrotoluene 19.99 165 58556 2.80 ug/l 93 22) Acenaphthylene 19.92 152 385780 3.48 ug/l 99 23) Acenaphthene 20.48 153 294462 3.86 ug/l 98 24) 2,4-Dinitrotoluene 21.15 165 71461 2.67 ug/l # 88 25) Diethylphthalate 21.91 149 366510 4.18 ug/l 98 26) 4-Chlorophenyl-phenylether 22.03 204 143526 4.04 ug/l 100 27) Fluorene 22.00 166 314898 4.07 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 22.49 77 363432 3.50 ug/L 98 (#) = qualifier out of range (m) = manual integration REFB.D GCMS0103.M Thu Jan 10 09:17:26 2002 Page 1 NYC-WTC_000017539