Reference data sheet from the DEP laboratory documenting GCMS analysis parameters and results for volatile organic compounds.
NYC-WTC_000017054–000017059Folder label: “GCMS X 12/14/01 A 1/1/02”
OCR status: ocr · source: ours
NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) 7 Data File : C:\HPCHEM\1\DATA\DEC3101\REFC.D Vial: 16 Acq On : 1 dan 2002 1:33 am Operator: 209 GALOS Sample : gems scan 12/14a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 11:41 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator! Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev(Min 1) 1,4-Dichlorobenzene-d4 11.68 152 830002 20.00 ug/l -0.02 10) Naphthalene-ds 15.28 136 3242639 20.00 ug/l -0.03 17) Acenaphthene-d10 20.55 164 1644517 20.00 ug/l -0.02 29) Phenanthrene-d10 24.98 188 2296615m 20.00 ug/l -0.01 38) Chrysene-di2 33.02 240 1412442 20.00 ug/l -0.01 44) Perylene-d12 37.12 264 820756 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 30.06 235 134086 5.31 ug/ml 0.00 Spiked Amount 5.000 Recovery = 106.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.44 74 74506 2.04 ug/l # 68 3) bis(2-Chloroethyl) ether 11.11 93 187770 3.28 ug/l # 89 4) 1,3-Dichlorobenzene 11.58 146 117300 1.94 ug/1 97 5) 1,4-Dichlorobenzene 11.72 146 133691 2.19 ug/l # 98 6) 1,2-Dichlorobenzene 12.24 146 132863 2.36 ug/l 96 7) 2,2"-oxybis(1-Chloropropan 12.58 45 324942 4.45 ug/l # 93 8) N-Nitroso-di-n-propylamine 12.97 70 129895 3.98 ug/1 90 9) Hexachloroethane 13.06 117 38961 1.75 ug/l 88 11) Nitrobenzene 13.37 77 161748 3.20 ug/l # 85 12) Isophorone 14.01 82 381958 3.92 ug/l # 93 13) bis(2-Chloroethoxy)methane 14.70 93 212288 3.25 ug/l 97 14) 1,2,4-Trichlorobenzene 15.17 180 111410 2.37 ug/1 97 15) Naphthalene 15.34 128 467788 3.02 ug/l 100 16) Hexachlorobutadiene 15.89 225 36963 1.61 ug/l 96 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.86 162 249062 2.65 ug/1 96 20) Dimethylphthalate 19.96 163 358502 3.28 ug/1 99 21) 2,6-Dinitrotoluene 20.17 165 50745 1.97 ug/l # 55 22) Acenaphthylene 20.09 152 397567 3.02 ug/1 99 23) Acenaphthene 20.65 153 302191 3.21 ug/l 99 24) 2,4-Dinitrotoluene 21.39 165 48497 1.48 ug/l # 7 25) Diethylphthalate 22.08 149 388196 3.84 ug/l 98 26) 4-Chlorophenyl-phenylether 22.21 204 140499 3.18 ug/1 91 27) Fluorene 22.18 166 317085 3.28 ug/l 98 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 403182 3.86 ug/L # 87 (#) = qualifier out of range (m) = manual integration REFC.D GCMS1126.M Tue Jan 15 11:41:49 2002 Page 1 NYC-WTC_000017056
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NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
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Reference data sheet from the DEP laboratory documenting GCMS analysis parameters and results for volatile organic compounds.
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Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 31, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017898
Laboratory report documenting GCMS calibration data for sample AD30470 conducted on December 31, 2001.
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Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
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Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017537
Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016807
GCMS calibration report for sample AD30009 dated December 20, 2001, listing standard compound responses.
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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31017 performed on January 18, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016694
Reference standard analysis report verifying instrument performance for volatile organic compound testing in early 2002.
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Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049782
Calibration data report for GCMS analysis of sample AD29228 generated on January 3, 2002.
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NYC-WTC_000017040
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
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NYC-WTC_000017041
Verification document from the DEP laboratory confirming the completion of GCMS analytical procedures in January 2002.
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NYC-WTC_000017042
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for various organic compounds.
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NYC-WTC_000017050
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 31, 2001.
Filed in the same folder
NYC-WTC_000017060
Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD29931 using GCMS on January 18, 2002.
Filed in the same folder